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Lecturer(s)
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Moudrý Jan, doc. Ing. Ph.D.
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Course content
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Improving the knowledge of PhD students in the basics of analytical chemistry and Gaining an overview of modern techniques used in analytical chemistry. Errors of chemical analyzes, expression of results. Evaluation of results of instrumental methods. Sensitivity of devices. Limits of determination. Matrix effects and their compensation. Equilibria of proteolytic, complexing, redox equilibria in solutions of sparingly soluble compounds. Chromatographic methods. Principle of chromatographic methods, their division. Liquid chromatography. Theoretical foundations, distribution constant, efficiency of chromatographic process and its expression. Principles of gas chromatography. Optical methods of chemical analysis. General principles, components of optical instruments. Emission spectral analysis, principles, use in practice. Absorption methods. Absorption spectrophotometry in the field of visible and ultraviolet radiation. Infrared spectrometry. Mass spectrometry. Electroanalytical methods. Potentiometric methods, ion selective electrodes, their construction and use. Voltammetric dissolution polarography. Electromigration methods. Electrophoresis, basic principles, working technique, devices. Isotachophoresis, principles, instrumentation.
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Learning activities and teaching methods
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Work with text (with textbook, with book), Individual preparation for exam, Work with multi-media resources (texts, internet, IT technologies), Individual tutoring
- Semestral paper
- 50 hours per semester
- Preparation for exam
- 50 hours per semester
- Class attendance
- 50 hours per semester
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Learning outcomes
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The aim is to gain an overview of modern techniques used in analytical chemistry.
Improving the knowledge of the basics of analytical chemistry. Gaining an overview of modern techniques used in analytical chemistry. compounds. Chromatographic methods. Absorption spectrophotometry in the field of visible and ultraviolet radiation. Infrared spectrometry. Mass spectrometry. Electroanalytical methods. Potentiometric methods. Voltammetric dissolution polarography. Electromigration methods. Electrophoresis, basic principles, working technique, devices. Isotachophoresis, principles, instrumentation.
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Prerequisites
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Completion of a master's or engineering degree
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Assessment methods and criteria
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Oral examination, Written examination, Seminar work
Working with text Individual study for the exam Working with multimedia resources Individual consultations with the teacher Elaboration of a seminar work on a given topic Presentation of seminar work
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Recommended literature
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BARTUŠEK, M. Úvod do elektroanalytických metod. 1984. 104 s.. Praha: SPN, 1984.
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DVOŘÁK, J., KORYTA J.. Elektrochemie, 1983. 410 s.. Praha: Academia, 1983.
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CHURÁČEK, J. Analytická separace látek. 1990. 384 s.. Praha: Státní nakladatelství technické literatury, 1990. ISBN 80-03-00569-8.
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Churáček J. Pokroky v teorii a instrumentaci moderních analytických metod. 1988. 193 s.. Pardubice: Vysoká škola chemicko-technologická, 1988.
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CHURÁČEK, J. Úvod do vysokoúčinné kapalinové kolonové chromatograrie, 1984. 188 s.. Praha: SNTL - Nakladatelství technické literatury, 1984.
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KANICKÝ, V., OTRUBA V., SOMMER L., TOMAN J.. Optická emisní spektrometrie v indukčně vázaném plazmatu a vysokoteplotních plamenech. 1. st. , 1992. 152 s.. Praha: Academia, 1992. ISBN 80-200-0215-4.
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KORYTA, J. Současné trendy v elektrochemii. 1986. 128 s. Praha: Academia.
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SOMMER, L. Analytical absorption spectrophotometry in the visible and ultraviolet : the principles, 1989. 310 s.. Amsterdam: Elsevier, 1989. ISBN 0-444-98882-38.
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SOMMER, L. Analytická spektrometrie. 1986. 173 s.. Praha: Státní pedagogické nakladatelství, 1986.
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Zýka J. Analytická příručka. Díl I. 1988. 678 s.. Praha: SNTL - Nakladatelství technické literatury, 1988.
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Zýka J. Analytická příručka. Díl II, 1988. 831 s.. Praha: SNTL - Nakladatelství technické literatury, 1988.
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