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Lecturer(s)
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Křížek Martin, prof. Ing. CSc.
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Course content
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1. Sampling, sample handling 2. Sample decomposition and preparation prior to analysis 3. Classical detection methods, Fresenius system 4. Gravimetric methods, TGA, DTA 5. Aqueous solution equilibria 6. pH, calculations, activity, distribution coefficient 7. Buffer solutions, solving multiple equilibrium problems 8. Neutralization titrations 9. Oxidation/reduction titrations 10. Applications of redox titrations, complex-formation titrations 11. Precipitation titrimetry 12. Classical separation methods 13. Extraction 14. Ion exchange, statistics
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Learning activities and teaching methods
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Monologic (reading, lecture, briefing)
- Preparation for credit
- 80 hours per semester
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Learning outcomes
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The aim of the course is to provide a critical understanding, as well as theoretical knowledge of classical chemical analysis. The course begins with a theoretical section, which treats the basics of chemical analysis. The subsequent lectures are aimed at individual techniques of classical chemical analysis e.g. sampling and sample handling, aqueous solution equilibria, precipitate formation, complex formation, gravimetry, titrimetry. The course is included in teacher training programme and it is not finished by an examination as it forms an indivisible unit with Analytical Chemistry II.
Ability to comunicate with analytical workplaces, to understand the classical analytical results; ability to transformate knowledge of analytical chemistry to the school system; ability to apply knowledge in other chemical and related disciplines.
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Prerequisites
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No
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Assessment methods and criteria
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Oral examination
Commanding of the basics of selected parts of analytical chemistry with respect to the necessary understanding of inorganic, organic and physical chemistry.
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Recommended literature
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Harris,D.C. Quantitative chemical analysis. W.H.Freeman, 2016. ISBN 978-1-4641-3538-5.
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Křížek, M. Základy výpočtů v analytické chemii a základy práce s daty. JU Č.Budějovice, 2022. ISBN 978-80-7394-917-4.
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Křížek,M.-Šíma,J. Analytická chemie. JU Č.Budějovice, 2015. ISBN 978-80-7394-486-5.
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Miller,J.N-Miller,J.C. Statistics and Chemometrics for Analytical Chemistry. Pearson, 2018. ISBN 978-1-292-18671-9.
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Scholz,F. Chemical equilibria in analytical chemistry. Springer, 2019. ISBN 978-3-030-17179-7.
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Skoog,D.A. Analytická chemie. VŠCHT Praha, 2019. ISBN 978-80-7592-043-0.
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Tissue,B.M. Basics of analytical chemistry and chemical equilibria. Wiley, 2013. ISBN 978-0-470-59208-3.
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