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Lecturer(s)
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Křížek Martin, prof. Ing. CSc.
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Course content
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1. Differences between classical and instrimental analysis 2. Potentiometry, electrodes, pH measurement 3. Potentiometric titrations, ion selective electrodes 4. Conductivity measurements, electrolysis 5. Electrogravimetry, voltammetry 6. Polarography 7. Introduction to spectrochemical methods 8. Instruments for optical spectrometry 9. Atomic emission methods, molecular fluorescence spectroscopy 10. Atomic absorption methods, RTG spectrometry 11. Molecular absorption and infrared spectroscopy, MS 12. Chromatography, principles, TLC 13. Chromatography, GC, HPLC 14. Electromigration techniques, ITP, HPCE
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Learning activities and teaching methods
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Monologic (reading, lecture, briefing)
- Preparation for credit
- 100 hours per semester
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Learning outcomes
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The aim of the course is to provide a critical understanding, as well as theoretical knowledge of instrumental analytical chemistry. The course begins with a theoretical section, which treats the basics of instruments handling. The subsequent lectures are aimed at individual techniques: electroanalytical (potentiometry, ion selective electrodes, voltametry), spectroscopy (atomic, molecular) separation methods (chromatography, electrophoresis).
Ability to comunicate with istrumental analytical workplaces, to understand the instrumental results; ability to transformate knowledge of analytical chemistry to the school system; ability to apply knowledge in other chemical and related disciplines.
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Prerequisites
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No
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Assessment methods and criteria
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Oral examination
Commanding of the basics of selected parts of instrumental analysis with respect to the necessary understanding of physics and inorganic, organic and physical chemistry.
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Recommended literature
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Harris,D.C. Quantitative chemical analysis. W.H.Freeman, 2016. ISBN 978-1-4641-3538-5.
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Křížek, M. Základy výpočtů v analytické chemii a základy práce s daty. JU Č.Budějovice, 2022. ISBN 978-80-7394-917-4.
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Křížek,M.-Šíma,J. Analytická chemie. JU Č.Budějovice, 2015. ISBN 978-80-7394-486-5.
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Miller,J.N-Miller,J.C. Statistics and Chemometrics for Analytical Chemistry. Pearson, 2018. ISBN 978-1-292-18671-9.
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Scholz,F. Chemical equilibria in analytical chemistry. Springer, 2019. ISBN 978-3-030-17179-7.
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Skoog,D.A. Analytická chemie. VŠCHT Praha, 2019. ISBN 978-80-7592-043-0.
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Tissue,B.M. Basics of analytical chemistry and chemical equilibria. Wiley, 2013. ISBN 978-0-470-59208-3.
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