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Lecturer(s)
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Šíma Jan, doc. RNDr. Ph.D.
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Course content
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Introduction 2.Qualitative analysis - identification of cations 3. Gravimetric determination of iron 4. Acidimetry - preparation of standard solution , determination of total alkalinity of technical hydroxide 5. Chelatometry - determination of magnesium and calcium ions in drinking water 6. Precipitation titrations - argentometry , indirect titration 7. Iodometry and bromometry - determination of ascorbic acid in Celaskon pellet 8. Permanganometry - preparation of standard solution , determination of FeSO4 in medical drug 9. Potentiometry - determination of chlorides with using ion selective electrode 10. Spectrophotometry - determination of Fe3+ with using rhodanide
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Learning activities and teaching methods
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Dialogic (discussion, interview, brainstorming), Skills training, Laboratory
- Preparation for classes
- 15 hours per semester
- Preparation for credit
- 15 hours per semester
- Class attendance
- 28 hours per semester
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Learning outcomes
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Laboratory practices of analytical chemistry was constituted as a continuation of Analytical chemistry lecture. Practical training is focused on classical analytical chemistry method (qualitative analysis, gravimetric and volumetric determinations). The subject also includes some of the most common instrumental analytical methods (potentiometry, conductometry, spectrophotometry).
Ability to understand praktical aspects of chemical and instrumental methods and to solve analytical problems.
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Prerequisites
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Theory of analytical chemistry
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Assessment methods and criteria
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Student performance assessment, Analysis of student's work activities (technical works), Systematic student observation, Test, Development of laboratory protocols
Theoretical knowledge of basic and instrumental analytical techniques.
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Recommended literature
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Holzbecher Z., Churáček J. Analytická chemie. Praha SNTL, 1987.
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Křížek M., Jírovcová E. Cvičení z anorganické a analytické chemie. České Budějovice, 2010.
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Křížek,M. Základy výpočtů v analytické chemii, skriptum JU,. 2001.
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Křížek,M.-Šíma,J. Analytická chemie. JU, 2015. ISBN 978-80-7394-486-5.
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Opekar F., Jelínek I., Rychlovský P., Plzák Z. Základní analytická chemie. Praha, Karolinum, 2002.
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Zýka J. Analytická příručka I a II. Praha SNTL, 1988.
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